Bleach Volume 66

The zombified Hitsugaya easily defeats Ikkaku, Yumichika and Charlotte, facing Mayuri alongside the zombified versions of Rangiku, Kensei, and Rose. But Mayuri manages to call in his resurrected Arrancar, and face the zombified trio with ease. And later injects two of them with his modified blood to free them from Giselle's control, and make them his own. As she is defeated. Meanwhile, after an unseen battle with Byakuya fighting against the three Sternriiter members, "N" Robert Accutrone, "T" Candice Catnipp and "U" NaNaNa Najahkoop, Sternritter "L" PePe Waccabrada uses his ability to control Hisagi and Meninas before overpowering Byakuya while attempting to take out Liltotto. But Byakuya is quickly saved by Mayuri as he has Kensei defeat Pepe who finds himself eaten by a vengeful Liltotto. In the Soul King Palace, Tenjiro is unable to attack Yhwach due to interference from Sternritter "W" Nianzol Weizol prior to the Sternritter's death by Senjumaru Shutara. After that, Yhwach reveals his elite guard: Sternritters "M" Gerard Valkyrie, "X" Lille Barro, "C" Pernida Parnkgjas and their newest member, Sternritter "D" Askin Nak Le Varr. Though Lille kills Senjumaru and destroys the palace, it is revealed to an illusion as the other Royal Guards join the battle with Ōetsu swiftly killing off all Yhwach's bodyguards save Askin who subjects Ōetsu to his ability.

Sorry I Am Strong
Contains chapters 592 - 601.