Bleach Volume 34

When Neliel attempts to finish off Nnoitora, she transforms back into her child form. Ichigo tries to help Nel, but almost killed by Tesla when Kenpachi Zaraki intervenes. Telling Ichigo not to interfere in his fight against Nnoitora, Kenpachi reveals that Urahara made the entrance into Hueco Mundo stable enough for the captains to enter: Retsu Unohana saves Chad and Gantenbainne from the Exequias. Byakuya reaches Rukia as she was about to be killed by Séptima Espada Zommari Rureaux, who he kills when the Espada whose Rukia's body like a puppet to fight him. Renji, Uryū and Nel's Fracciones are saved by Mayuri, who stops Szayel's techniques. Mayuri initially seems unable to fight back against Szayelaporro, but he reveals that placed a bacteria in Uryū that allow him to learn of the voodoo dolls and counter them. Mayuri then activates his bankai and has it swallow Szayelaporro. Though Szayelaporro resurrect himself by absorbing Nemu's spiritual particles through his Gabriel technique while turning Mayuri's bankai against him. However, Szayelaporro learns too late that he ingested a "superhuman" drug inside Nemu's body that increases his senses to the point where his body cannot respond to the overstimulation, leaving him at Mayuri's mercy as he stabs the immobilizes Espada in the heart.

King of The Kill
Contains chapters 296 - 305.